A rare gamma-pyranopyrazole skeleton: design, one-pot synthesis and computational study


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Ucuncu M., Canturk C., Karakus E., Zeybek H., BOZKAYA U., Soydas E., ...More

ORGANIC & BIOMOLECULAR CHEMISTRY, vol.14, no.31, pp.7490-7494, 2016 (SCI-Expanded, Scopus)

Abstract

Drawing upon a consecutive amide coupling and intramolecular cyclisation pathway, a one-pot, straight-forward synthetic route has been developed for a range of pyrazole fused gamma-pyrone derivatives. The reaction mechanism proposed for the chemoselective formation of gamma-pyranopyrazole is furthermore fully supported by experimental and computational studies.