2025 AIAA SciTech Forum and Exposition, Orlando, Amerika Birleşik Devletleri, 6 - 10 Ocak 2025, cilt.1, ss.1-7, (Tam Metin Bildiri)
Metal organic framework (MOF) crystalline structures have emerged as promising materials due to their exceptional porosity and surface area. This study focuses on the solvothermal synthesis of MIL-125 nanoparticles, a specific MOF structure. A systematic investigation was conducted to explore the influence of key synthesis parameters, including residence time, temperature, precursor concentration, and reactor size, on the formation and properties of MIL-125 nanoparticles. By manipulating the nucleation window, defined by the interplay of thermodynamic and kinetic factors, we achieved well-defined, crystalline MIL-125 nanoparticles with tailored properties. Our findings provide valuable insights into optimization of MIL-125 synthesis to control the crystallinity and properties of the resulting MOF material for potential applications in catalysis, gas storage, sensing, and drug delivery.