Electrochemistry of poly(5-phenyl dipyrromethane) and its characterization


BOLAT G. , Kuralay F., TEMELLİ B. , ÜNALEROĞLU C. , ABACI S.

POLYMER BULLETIN, cilt.72, ss.867-879, 2015 (SCI İndekslerine Giren Dergi) identifier identifier

  • Cilt numarası: 72 Konu: 4
  • Basım Tarihi: 2015
  • Doi Numarası: 10.1007/s00289-015-1311-x
  • Dergi Adı: POLYMER BULLETIN
  • Sayfa Sayıları: ss.867-879

Özet

In this work, electropolymerization of 5-phenyl dipyrromethane (DPM) and electrochemical behavior of the obtained polymer were performed. The monomer was electropolymerized in a solution of DPM and 0.1 M tetra-n-butyl ammonium perchlorate/dichloromethane supporting electrolyte/solvent solution system on a Pt electrode by cyclic voltammetry technique. The polymeric film was then characterized by scanning electron microscopy, atomic force microscopy, fourier transform infrared-attenuated total reflectance, nuclear magnetic resonance spectroscopy, differential scanning calorimetry and alternative current impedance techniques.